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Título: | Simultaneous multi-mycotoxin determination in maize and poultry feeds from Brazil by liquid chromatography/tandem mass spectrometry |
Autor(es): | Souza, Maria de Lourdes Mendes de Sulyok, Michael Freitas-Silva, O. Costa, Sônia Soares Brabet, Catherine Machinski Junior, Miguel Sekiyama, Beatriz Leiko Vargas, Eugenia Azevedo Krska, Rudolf Schuhmacher, Rainer |
Data: | 9-Set-2009 |
Citação: | Souza, Maria de Lourdes Mendes de; Sulyok, Michael; Freitas-Silva, O.; Costa, Sônia Soares; Brabet, Catherine; Machinski Junior, Miguel; Sekiyama, Beatriz Leiko; Vargas, Eugenia Azevedo; Krska, Rudolf; Schuhmacher, Rainer, Simultaneous multi-mycotoxin determination in maize and poultry feeds from Brazil by liquid chromatography/tandem mass spectrometry. ISM Conference 2009 - Worldwide Mycotoxin Reduction in Food and Feed Chains. Tulln, Austria, Sep. 9-11, 175-175, 2009. |
Resumo(s): | A multi-mycotoxin method based on High Performance Liquid Chromatography coupled with tandem Mass Spectrometry detection (HPLC-MS /MS) was applied to investigate the occurrence of toxic fungal metabolites in samples collected from a poultry feed factory and integrated poultry farms, in Brazil. A total of 119 samples were analyzed including 38 maize grain samples collected from the factory reception, 36 maize grain samples and 9 maize by- product samples collected during the factory processing, and 36 poultry feed samples collected from poultry farms. Twenty mycotoxins were detected and quantified in the investigated samples: aflatoxins B 1 , B2, G 1 , G2, fumonisins B 1 , B2 and B3, hydrolyzed fumonisin B 1 , zearalenone, agroclavine, chanoclavine, deoxynivalenol, nivalenol, enniatin A, A I , B, B,, beauvericin, kojic acid and moniliformin. All samples were contaminated with fumonisins B 1 , B2 and B3. Contamination levels were low (near the LOD) most of toxins, except for FB I and FB 2 that reach 6,000 mg.mU l and 2,450 mg.mL"' in maize and 1,120 mg.mL"' and 54 mg.mL" 3 in feed, respectively. This is the first study dealing with agroclavine, chanoclavine, enniatin A, A 1 , B, B 1 , beauvericin and kojic acid contamination of maize and poultry feeds from Brazil. |
Tipo: | Resumo em ata de conferência |
URI: | https://hdl.handle.net/1822/38248 |
Arbitragem científica: | yes |
Acesso: | Acesso aberto |
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Ficheiros deste registo:
Ficheiro | Descrição | Tamanho | Formato | |
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document_26491_1.pdf | 1,27 MB | Adobe PDF | Ver/Abrir |