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https://hdl.handle.net/1822/44406
Título: | Synthesis of 1-(4-bromophenyl)-1H-pyrrole by Clauson-Kass reaction |
Autor(es): | Raposo, M. Manuela M. Castro, Maria Cidália Rodrigues Fernandes, Sara Sofia Marques |
Data: | 2016 |
Editora: | Royal Society of Chemistry |
Resumo(s): | The aim of this work is the synthesis of 1-(4-bromophenyl)-1H-pyrrole via the Clausson-Kass reaction, using simple experimental techniques and commercially available reagents. Several experimental techniques will be implemented including heating at reflux, liquid-liquid extraction, gravity and vacuum filtration, thin layer chromatography (TLC), and melting point determination. The determination of the structure of the compound synthesized will be also performed using 1H NMR spectroscopy techniques. The duration of the experiment is 2 sessions: session 1: preparation of 1-(4-bromophenyl)-1H-pyrrole; session 2: purification of 1-(4-bromophenyl)-1H-pyrrole. The difficulty level of this experiment is low and the level of study is medium. |
Tipo: | Capítulo de livro |
URI: | https://hdl.handle.net/1822/44406 |
ISBN: | 978-18-49739-63-4 |
Versão da editora: | http://pubs.rsc.org/en/content/ebook/978-1-84973-963-4#!divbookcontent |
Acesso: | Acesso restrito autor |
Aparece nas coleções: | CDQuim - Livros e Capítulos de Livros / Books and Book Chapters |
Ficheiros deste registo:
Ficheiro | Descrição | Tamanho | Formato | |
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Chapter 222, Experiment 17.5., p. 1011-1014 -Synthesis of 1-(4-bromophenyl)-1H-pyrrole by Clauson-Kass reaction.pdf Acesso restrito! | 186,73 kB | Adobe PDF | Ver/Abrir |