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TitleA Ugi multicomponent reaction in the synthesis of N-cyclohexyl-2-(N-(4-methoxybenzyl)acetamido)-2-(thien-2’-yl)acetamide
Author(s)Costa, Susana P. G.
Raposo, M. Manuela M.
Esteves, Cátia Isabel Canavezes
KeywordsAmino acids
Multicomponent reaction
Ugi reaction
Organic chemistry experiments
Laboratory classroom
Issue dateDec-2016
PublisherRoyal Society of Chemistry
CitationComprehensive Organic Chemistry Experiments for the Laboratory Classroom (COCELC), 2016, Cap. 111, Experiment, p 493-496
Abstract(s)The aim of this work is the synthesis of a protected unnatural amino acid using a Ugi multicomponent reaction, namely N-cyclohexyl-2-[N-(4-methoxybenzyl)acetamido]-2-(thien-2-yl)acetamide. Several experimental techniques will be considered such as thin-layer chromatography (TLC), vacuum filtration, and column chromatography on silica gel. The determination of the structure of the compound synthesized will be performed by NMR spectroscopy.
TypeBook part
Publisher version
AccessRestricted access (Author)
Appears in Collections:CDQuim - Livros e Capítulos de Livros / Books and Book Chapters

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